• Hong Kong Biodiesel Specification work has been completed

• Work has been initiated to complete testing requirements of the  European Union Bio-diesel Specification

• The new bio-diesel standard recently introduced in Australia -- Australian Fuel Standard (Biodiesel) Determination 2003 is based on the United States  Standard /Specification and  European Biodiesel Standard/Specification.  Work has been started to comply with the Commonwealth of Australia’s testing  requirements.

• A client was required to be compliant with USCL METHOD 34-07  or USCL METHOD 34-08 - Quantitation of Paraffin in Imported Wax as U.S.Customs laboratory analyses of imported candles have revealed that a large percentage of samples which claim to contain under 50% petroleum wax, were found to have over 50% petroleum wax.  The department of Commerce (DOC) has found similar results in their tests.  Therefore, they are requiring independent laboratory reports when the claim is made that candles contain under 50% petroleum wax (that is, for example, that they contain over 55% "palm oil wax").  These methods are applicable to the determination of the total amount of paraffin type hydrocarbons in a wax sample. These results can then be used to determine the total amount of paraffin wax added to articles of wax.  This method can also be used to qualitatively detect the presence of waxes other than paraffin and beeswax in articles of wax by comparison with other reference chromatograms.   [Reference:  Department of the Treasury, United States Customs Service - Request for Information - - Customs Form 28 (102591).]

• Reformulation of finished gear lube to change additive suppliers

• Grease contamination analyses and cone penetration determination

• Standard Specification for Industrial Burner Fuels from Used Lubricating Oils, the Standard Specification for Fuel Oils, the Standard Specification for Diesel Fuel Oils, and the Standard Specification for Gas Turbine Fuel Oils

• #1 Diesel Fuel [No 1 Diesel Fuel] Analysis performed for Rush compliance

• #2 Diesel Fuel [No 2 Diesel Fuel] Analysis performed for Rush compliance

• #5 Diesel Fuel [No 5 Diesel Fuel] Analysis performed for Rush compliance

• Grades RF04, RF05L, RF05H, and RF06 -- used lubricating oil blends analyzed for use in industrial burners -- Grades 1, 1 Low Sulfur, 2 and 2 Low Sulfur --middle distillate fuels

• pH of a hazardous waste liquid, sludge, semisolid and solid

• Grades of fuel oil for use in various types of fuel-oil-burning equipment

• A special low-sulfur grade kerosene suitable for use in nonflue-connected kerosene burner appliances

• Refractometer -- precision optical instrument designed to measure the concentration or mixture ratio of water soluble fluids -- used to perform Refractive Index analysis

• Dean Stark water run per manufacturer's requirement

• Biodiesel Fuel (B100) Blend Stock for Distillate Fuels per ASTM D6751 completed

• British Thermal Unit [btu] content requested on paper 

• Used Lubricating Oils analyzed for Industrial Burner Fuels

• Palm Oil content of gel candles determined for import regulations

• Gum base for chewing gum FDA 21CFR178 compliance testing

• Bio-diesel  required testing, based on the ASTM Designation: PS 121-99, Provisional Specification for Bio-Diesel Fuel  (B100) Blend Stock for Distillate, including Flash Point, Acid Number, Sediment and Water, and Free and Total Glycerin [ASTM D6584]

• FDA, 21CFR178.3260 Parts B and C for compliance for indirect food contact.

•  Particle Count and Particle Size determinations proved filtration currently in place was underutilized

• Distillation data provided an independent petroleum producer with invaluable information to sell their crude oil at the highest price.

• Composition of corrosion on safety harnesses determined

• Modified Ames run to determine carcinogenic effects on multiple products

• Cetane Index performed on line of diesel fuels

• Flash Points on Fisher Tropsch wax

• Characterization simulations run on new formulation

• Sulfur extractions performed on yarn, fabric and cloth

•  Investigative study on Machinable [Machineable] Wax -- mold release cracking

• Compliance Testing completed for a newly developed product.

• Provisional Specifications for Biodiesel Fuel (B100) Blend Stock for Distillate Fuels [PS-121-99] provided for a blending facility

• Hydraulic Fluid formulations were re-evaluated for a customer who wanted to change additive supplier.

• Arsenic determination of water. wastewater and soil samples was fine-tuned to handle a clients governmental requirements.

• A major airline needed RAPID de-icer data on a routine basis.  We developed an antifreeze [anti-freeze] - ethyl glycol - ICP procedure to exceed their expectations.

• Analyzed fabric - textile - felt for characteristics, including tarnish

• Developed a customized used oil analysis maintenance program for the locomotive engines used by a national railroad.

• Compliance with The National Fire Protection Association's National Fire Codes ® the "NFPA Hazard Diamond" Rating was completed for major manufacturer's product line.

• Assisted an Eastern pharmaceutical company in developing a new product.

• An unknown gel-like substance was identified in a turbine oil filter line for   Quality  Assurance and OSHA compliances.

• Vendor needed assurance of compliance of LPG with HD-5 of GPA Standard   2140 and ASTM D-1835.

• Karl Fisher water was run on forklift hydraulic fluids to help determine the     cause of equipment problems.

• Evaluate sample for CAM 17 metals [ California Administrative Manual] in conjunction with EPA Method 6010 and CCR Title 22

• Detailed examination of toner for possible contamination

• Comprehensive evaluation of rolling oil in metal working facility.

• Analytical composition of refreezeable liquid was determined for a major      plastic manufacturer

• Elemental composition  of  Collidial Silver solution

• Study of non-petroleum oils (palm oil, soybean, etc.) as possible alternatives       to fossil fuel based products.

• Flash Points and NFPA rating performed on various process streams for insurance rating.

• Recycled Fuel Oil analyzed for compliance with standard ASTM D-6448

• Contract development of elemental tracers in lubricant fluids that could be  carried over with fluid changes.

• Institute of Petroleum method, IP 346 for the determination of  polycyclic aromatics was run on wax samples for a European wax compounder 

• API [American Petroleum Institute] testing, Part B certification was completed.

•  Consultant needed assistance completing a MSDS [Material Safety Data Sheet].

•  Water analysis determined EPA maximum contamination levels were within limits. 

• Wax analysis required in 21 CFR 172.886 for FDA Part 1 approval was run

• Peroxide Number were needed on wax samples to be shipped overseas  

•   PONA determinations were run on gasoline samples from a major supplier

• A major crude purchaser requested Salts in Crude Oil, ASTM D-3230-99

•  Additive supplier had changed and reformulations were completed.

•  Coliform bacteria was present in a suburban homeowner's  water well system

• Sulfate content is monitored for a local chrome plating corporation

• A pharmacologist in the biotechnical industry needed data on a compound for use in organic synthesis

• Quality control protocol and quality control assurance procedures were established for a foot soak manufacturer

• Elemental analysis of kerosene to determine fuel quality.

•  Insulation material was determined to be asbestos free.

•  Melting point of wax determined for a leading candle manufacturer

• Analysis of gasoline storage tank determined that contamination was present

•  A sample of Dead Sea mud was received for compositional analysis.

• Food and Drug Administration - FDA Shelf-Life was determined for a new food product

• Fuel dilution was present in used diesel engine oil, the quick discovery enabled the customer to save a costly maintenance bill.

•  The contents of relish were determined for a client

•  FDA ISO 9001 compliance was completed for a new food manufacturer

•  A major importer noticed a distinct chemical odor in shirts.  Odorant analysis proved contaminants were present.

• Material Data Safety Sheets [ MSDS's ] were completed for Bath Salts and Body Lotions for a new line of products

• Hydraulic oil formulations revised to meet specifications

•  A plastic manufacturer, pursuing a new international market, was in need of a 200-elemental analysis to complete a required European Substance Declaration for exporting the product

• A major petroleum refinery needed arsenic tested in recent crude purchases

•  An importer was in need of a  Toxic Substance Declaration required by TSCA Toxic Substances Control Act Certification [19 CFR 12.121 ], Declarations for toxic substances.

•  A state official wanted to develop an ethanol in groundwater testing program and complete a procedure development study.

• An independent lubricant blender wanted to do a comparison cost study on varied additives and their affect on formulations and re-formulations.

• An international client needed Department of Transportation DOT 4 certification for brake fluid.

•  A municipality needed data for their watershed project

•  A fleet manager needed a comprehensive study of used oil, coolant and antifreeze

•  A contractor was in need of hazardous content in soil samples

• A grandfather was concerned about possible lead-based paint residue in his new grandson's bedroom

• A capital venturist wanted an independent laboratory to confirm test data

• A homeowners wanted data on their water well system, before new construction was started on an adjoining property

•  A independent consultant needed data in part per billion as to the content of arsenic in crude oil for their client

• A plant manager wanted to check the condition of the company's catalyst

• A CEO was in need of an independent laboratory to assure optimum savings on additive purchases

•  A realtor needed multiple tests run on a property to meet lenders requirements.

•  A laboratory manager needed immediate backup for non-working instrument

• A division manager wanted to know if long-time employees were protecting their own interests or the companies

•  An architect needed to know if insulation contained asbestos

•  A small business was in need of a new wax meeting critical tolerances

• A quality control manager was questioning an additive specification

• An engineer needed alternatives to complete a crucial phase and "de-bottle neck" a current process

•  Corporate management needed technical expertise to stream-line, assess and evaluate, develop, and interpret data before investing in a new high-tech automated system within their strategic plan

•  A project manager needed assistance with data collection and interpretation

• The owner of an industrial complex needed technical advise to develop an integrated solution for future business changes

• A petroleum refiner wanted pilot simulations run on a newly formulated product

• Research and development activities halted after a takeover and new staffing was quickly needed.

• An entrepreneur needed a laboratory and wished to avoid major capital investment in experienced personnel and sophisticated instrumentation

• After a merger, management needed several laboratory assessments and advice on consolidating

• After a catastrophic storm, equipment failed and product contamination occurred.  Rapid results were needed to determine the extent of damage and out-servicing until repairs could be competed.

• New product development and quality assurance standards were needed to comply with environmental concerns. 

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